Kusamala Pogwiritsa Ntchito Hastelloy Alloy High-Pressure Reactors

1.Kuyika chilengedwe

TheHastelloyAuwu High Kupanikizika Rwoyimbaziyenera kuikidwa m'chipinda chogwiritsira ntchito choponderezedwa kwambiri chomwe chimakwaniritsa zofunikira zoteteza kuphulika. Ma reactors angapo a Hastelloy akagwiritsidwa ntchito, amayenera kuyikidwa padera, ndi ma reactor awiri aliwonse olekanitsidwa ndi khoma loteteza chitetezo kuphulika. Pazigawo zilizonse zopita kunja, onetsetsani kuti zidazo zili ndi mpweya wabwino pamaso pa zida zophulika.

2.Kutentha Kuganizira

Ngati kutentha kwamagetsi kwamafuta kumagwiritsidwa ntchito, onetsetsani kuti mwagula mtundu woyenera wamafuta otentha potengera kutentha kwa ntchito.

3.Kusindikiza Reactor

The riyakitala thupi ndi chivindikiro ayenera mwachindunji liniya kukhudzana ndi gasket kapena ndi conical ndi arcuate kusindikiza pamalo. Kumangitsa mtedza waukulu kumakanikiza pamodzi kuti apeze chisindikizo chogwira mtima. Mukamangirira, mtedzawo uyenera kutembenuzidwa mofananira komanso pang'onopang'ono m'magawo angapo kuti zitsimikizire ngakhale kukakamiza komanso kuteteza chivindikiro kuti chisapendekeke, potero kuonetsetsa chisindikizo choyenera.

Kuyika kwa 4.Valve ndi Gauge

Ikani ma valavu, zoyezera kuthamanga, ndi ma valve otetezera pomanga mtedza wofanana kuti mukwaniritse chisindikizo. Malo osindikizira a arcuate kumbali zonse ziwiri za kugwirizana sayenera kusinthasintha wina ndi mzake. Pakuphatikizana, zolumikizira zonse zolumikizidwa ziyenera kupakidwa mafuta - mwina ndi mafuta oyenera kapena osakaniza amafuta a graphite - kuti zisawonongeke.

5.Kuzizira Njira

Kuti aziziziritsa, madzi amatha kuzunguliridwa kudzera muzitsulo zoziziritsa mkati. Kuzizira kofulumira ndikoletsedwa kupewa kupsinjika kwambiri kwa kutentha komwe kumatha kusokoneza mazenera oziziritsa ndi thupi la reactor. Panthawi yogwira ntchito, ngati kutentha kwa riyakitala kupitirira 100 ° C, madzi ozizira ayenera kufalitsidwa kudzera mu jekete lamadzi pakati pa magnetic stirrer ndi chivindikiro cha riyakitala kuonetsetsa kuti kutentha kwa madzi kumakhalabe pansi pa 35 ° C, zomwe zimathandiza kupewa demagnetization ya maginito.

6.Post-Reaction Procedures

Zomwezo zikatha, choyamba lolani kuti riyakitala izizire, kenaka mutulutse mpweya wamkati kudzera mupaipi kuti muchepetse kuthamanga kwa mpweya. Musati disassemble riyakitala akadali apanikizika. Symmetrically kumasula mabawuti waukulu ndi mtedza, kuchotsa iwo, ndiye mosamala kutsegula ndi kuchotsa chivindikirocho, kuwayika pa choyimira.

Kusamalira ndi Kuyeretsa

Pambuyo pa opareshoni iliyonse, yeretsani riyakitala ndi madzi oyeretsera oyenera kuteteza dzimbiri zazinthu zazikulu. Chotsani zotsalira zilizonse pathupi la reactor ndi malo osindikizira. Nthawi zonse sungani zida zaukhondo.

Kuti mudziwe zambiri za ma laboratory-scale micro-reactors ndiHayi PlimbikitsaniRochita, omasukaCtipezeni.